ВОЛЬТАМПЕРОМЕТРИЧНИЙ МЕТОД АНАЛІЗУ ДЛЯ АРХЕОЛОГІЇ ТА МИСТЕЦТВОЗНАВСТВА (КОРОТКИЙ ОГЛЯД)
DOI: http://dx.doi.org/10.30970/vch.6701.080
Анотація
Огляд присвячено застосуванню вольтамперометричного методу аналізу для дослідження археологічних і мистецьких об’єктів (датуванню та ідентифікації барвників, пігментів, мінералів, металів, сплавів та продуктів їхньої корозії, визначення технологічних характеристик артефактів тощо). З цією метою зараз використовують чимало інструментальних методів, які коротко згадано в огляді, серед яких вольтамперометричний аналіз починає набувати популярності. Для аналізу мистецьких та археологічних артефактів придатним є сучасний різновид вольтамперометрії – метод іммобілізованих частинок (VIMP), на якому в цій праці зосереджено особливу увагу. Зокрема, описано принципи методу, особливості підготовки проб і різновиди індикаторних електродів, які використовують для аналізу зразків культурної спадщини. Розглянуто приклади застосування VIMP для якісного та кількісного аналізу, автентифікації й датування пам’яток різного походження. Обґрунтовано перспективи розвитку VIMP як мікродеструктивного інструменту археометрії та мистецтвознавства.
Перша авторка – студентка Вікторія Рибак, ініціаторка та головна виконавиця написання цього огляду, – надихнулася до цієї праці дисципліною вільного вибору “Аналіз хімічний для археологів та мистецтвознавців”. Дисципліну викладають на кафедрі аналітичної хімії хімічного факультету, вона є відкритою для відвідування студентами всіх факультетів Університету. Тематика праці має міждисциплінарний характер та буде корисною для ознайомлення причетним до хімії, історії, археології, мистецтвознавства, а також усім охочим, адже автори мали намір доступно та стисло викласти інформацію з предмета, що є дуже обширним. Окрім того, наголошуємо на дефіциті літератури українською мовою, присвяченої суміжним тематикам.
Огляд містить понад дев’яносто літературних посилань щодо хімічного аналізу в археології та мистецтвознвстві, зокрема використання вольтамперометричного методу аналізу, серед них монографії, оглядові статті та оригінальні праці.
Ключові слова: вольтамперометричний аналіз, електрохімія, археологія, мистецтвознавство, артефакт.
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Doménech A., Sánchez S., Yusá M. D., Gimeno-Adelantado J. V., Bosch-Reig F., Saurí M. C. Electrochemical determination of the Fe(III)/Fe(II) ratio in archaeological ceramic materials using carbon-paste and composite electrodes // Electroanalysis. 2002. Vol. 14, No. 10. P. 685–696. DOI: https://doi.org/10.1002/1521-4109(200205)14:10<685::AID-ELAN685>3.0.CO;2-4
Doménech-Carbó A., Doménech-Carbó M. T., Gimeno-Adelantado J. V. Quantitation of metal ions in archaeological glass by abrasive-stripping square-wave voltammetry using graphite/polyester composite electrodes // Electroanalysis. 2003. Vol. 15, No. 4. P. 295–302. DOI: https://doi.org/10.1002/elan.200302716
Doménech-Carbó A., Doménech-Carbó M. T., Saurí-Peris M. C. Electrochemical identification of flavonoid dyes in solid work of art samples by abrasive voltammetry at paraffin-impregnated graphite electrodes // Talanta. 2005. Vol. 66, No. 3. P. 769–782. DOI: https://doi.org/10.1016/j.talanta.2004.12.034
Doménech A., Doménech-Carbó M. T., Osete-Cortina L. Electrochemical characterization of archaeological tin-opacified lead-alkali glazes and their corrosion processes // Electroanalysis. 2005. Vol. 17, No. 19. P. 1959–1969. DOI: https://doi.org/10.1002/elan.200503322
Doménech A., Doménech-Carbó M. T., Vazquez de Agredos Pascual M. L. Dehydroindigo: a new piece into the Maya Blue puzzle from the voltammetry of microparticles approach // J. Phys. Chem. B. 2006. Vol. 110, No. 12. P. 6027–6039. DOI: https://doi.org/10.1021/jp057301l
Doménech-Carbó M. T., Doménech-Carbó A., Osete-Cortina L., et al. A study on corrosion processes of archaeological glass from the Valencian region (Spain) and its consolidation treatment // Microchim. Acta. 2006. Vol. 154. P. 123–142. DOI: https://doi.org/10.1007/s00604-005-0472-y
Doménech-Carbó A., Doménech-Carbó M. T., Gimeno-Adelantado J. V., Bosch-Reig F. H-point standard addition method applied to solid-state stripping voltammetry: quantitation of lead and tin in archaeological glazes // Anal. Bioanal. Chem. 2006. Vol. 385, No. 8. P. 1552–1561. DOI: https://doi.org/10.1007/s00216-006-0597-9
Bosch-Reig F., Doménech-Carbó A., Doménech-Carbó M. T., Gimeno-Adelantado J. V. H-point standard addition method applied to voltammetry of microparticles: quantitation of dyes in pictorial samples // Electroanalysis. 2007. Vol. 19, No. 15. P. 1575–1584. DOI: https://doi.org/10.1002/elan.200703869
Doménech-Carbó A., Doménech-Carbó M. T., Peiró-Ronda M. A. Dating archaeological lead artifacts from measurement of the corrosion content using the voltammetry of microparticles // Anal. Chem. 2011. Vol. 83, No. 14. P. 5639–5644. DOI: https://doi.org/10.1021/ac200731q
Doménech-Carbó A., Doménech-Carbó M. T., Mas-Barberá X. Identification of lead pigments in nanosamples from ancient paintings and polychromed sculptures using voltammetry of nanoparticles/atomic force microscopy // Talanta. 2007. Vol. 71, No. 4. P. 1569–1579. DOI: https://doi.org/10.1016/j.talanta.2006.07.053
Doménech-Carbó A., Doménech-Carbó M. T., Capelo S., Pasíes T., Martínez-Lázaro I. Dating archaeological copper/bronze artifacts by using the voltammetry of microparticles // Angew. Chem. Int. Ed. Engl. 2014. Vol. 53, No. 35. P. 9262–9266. DOI: https://doi.org/10.1002/anie.201404522
Doménech-Carbó A., del Hoyo-Meléndez J. M., Doménech-Carbó M. T. Electrochemical analysis of the first Polish coins using the voltammetry of immobilized particles // Microchem. J. 2017. Vol. 130. P. 47–55. DOI: https://doi.org/10.1016/j.microc.2016.07.020
Doménech-Carbó A., Donnici M., Álvarez-Romero C., et al. Multiple-scan voltammetry of immobilized particles of ancient copper/bronze coins // J. Solid State Electrochem. 2021. Vol. 25. P. 195–206. DOI: https://doi.org/10.1007/s10008-020-04770-4
Martínez B., Piquero-Cilla J., Montoya N., et al. Electrochemical analysis of gold embroidery threads from archeological textiles // Solid State Electrochem. 2018. Vol. 22. P. 2205–2215. DOI: https://doi.org/10.1007/s10008-018-3927-x
Di Turo F., Mai C., Haba-Martínez A., Doménech-Carbó A. Discrimination of papers used in conservation and restoration by the means of the voltammetry of immobilized microparticles technique // Anal. Methods. 2019. Vol. 11. P. 4431–4439. DOI: https://doi.org/10.1039/C9AY00998A
Doménech-Carbó A., Doménech-Carbó M. T., Álvarez-Romero C., Pasíes T., Buendía M. Screening of Iberian coinage in the 2th–1th BCE period using the voltammetry of immobilized particles // Electroanalysis. 2019. Vol. 31. P. 1164–1173. DOI: https://doi.org/10.1002/elan.201900090
Saleh S. M., El‑Badry A. E. H. A., Abdel‑Karim A. M. Evaluation of the corrosion resistance of bronze patina or/and protective coating on the surface of the archaeological coins // Sci. Rep. 2025. Vol. 15. P. 2361. DOI: https://doi.org/10.1038/s41598-025-85290-x
Di Turo F., De Vito C., Coletti F. et al. Modeling solid-state reaction processes: application for the archaeometric study of potteries from Venus Fisica Temple in Pompeii (Italy) // J. Solid State Electrochem. 2025. Vol. 29. P. 41–50. DOI: https://doi.org/10.1007/s10008-024-06011-4
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