АЛМАЗНИЙ ЕЛЕКТРОД, ДОПОВАНИЙ БОРОМ В АНАЛІТИЧНІЙ ХІМІЇ: СПОСОБИ АКТИВАЦІЇ ПОВЕРХНІ ЕЛЕКТРОДА (КОРОТКИЙ ОГЛЯД)

O. Dushna, L. Dubenska, M. Vojs

Анотація


Огляд присвячено особливостям використання алмазного електрода, допованого бором (АДБЕ), в аналітичній хімії. АДБЕ – один з найсучасніших пристроїв для вольтамперометрії, який набуває щоразу більшої популярності для визначення слідових кількостей органічних речовин у складних об’єктах. Зараз використовують стрижневі (дискові) і плівкові АДБЕ. Головну увагу в огляді зосереджено на особливостях активації поверхні АДБЕ для використання в аналізі. Активують поверхню електрода потенціостатично, гальваностатично та в динамічних умовах, використовують різні фонові електроліти. Електрохімічно обробляють АДБЕ зазвичай у водних розчинах, здебільшого поверхня електрода одночасно очищується й активується. Правильне попереднє електрохімічне оброблення може бути цінним способом досягнення поліпшених аналітичних властивостей методики вольтамперометричного визначення. Отримують інтенсивніший аналітичний сигнал, вужчий, чіткіший пік та/або корисне зміщення потенціалу піка, що сприяє підвищенню чутливості і селективності визначення.

Огляд містить понад 80 літературних посилань щодо особливостей активації поверхні АДБЕ, серед них монографії, оглядові статті та оригінальні праці.

 

Ключові слова: вольтамперометрія, алмазний електрод, допований бором, активація поверхні, поляризація.


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Pınar P., Sentürk Z. Electrochemical and analytical performance of cathodically pretreated boron-doped diamond electrode for the determination of oxazolidinone antibiotic linezolid in cationic surfactant media // J. Electroanal. Chem. 2020. Vol. 878, No. 11468. DOI: https://doi.org/10.1016/j.jelechem.2020.114681

Hoshyar S., Barzani H., Yardım Y., Sentürk Z. The effect of CTAB, a cationic surfactant, on the adsorption ability of the boron-doped diamond electrode: application for voltammetric sensing of Bisphenol A and Hydroquinone in water samples // Colloids Surf. A Physicochem. Eng. Asp. 2021. Vol. 610, No. 125916. DOI: https://doi.org/10.1016/j.colsurfa.2020.125916

Allahverdiyeva S., Yardım Y., Sentürk Z. Electrooxidation of tetracycline antibiotic demeclocycline at unmodified boron-doped diamond electrode and its enhancement determination in surfactant-containing media // Talanta. 2021. Vol. 223, No. 121695. DOI: https://doi.org/10.1016/j.talanta.2020.121695

Pinar P. T., Yardim Y., Şentürk Z. Square-wave voltammetric sensing of Lawsone (2-hydroxy-1,4-naphthoquinone) based on the enhancement effect of cationic surfactant on anodically pretreated boron-doped diamond electrode // Acta Chim. Slov. 2021. Vol .68, No. 4. P. 1027–1032. DOI: https://doi.org/10.17344/acsi.2020.6617




DOI: http://dx.doi.org/10.30970/vch.6301.153

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